Oct 1, 2022 · Results from X-ray Photoelectron Spectroscopy (XPS) of molybdenum oxide samples are presented to elucidate how Mo (VI) oxide evolves to Mo (IV) oxide upon heating of a MoO 3 sample.

The XPS Spectra section provides raw and processed survey spectra, chemical state spectra, BE values, FWHM values, and overlays of key spectra. Atom% values from surveys are based on sample, as received, and Scofield cross-sections. Atom% values are corrected for IMFP and PE. Peak-fits are guides for practical, real-world applications.

Feb 1, 1996 · The surface properties of Mo oxides (MoO 2 and MoO 3) were investigated using X-ray photoelectron spectroscopy (XPS). As-prepared MoO 3 showed two well resolved spectral lines at 232.5 and 235.6 eV, which were assigned to …

Nov 5, 2018 · Here we used operando near-ambient pressure X-ray photoelectron spectroscopy to reveal important differences in the Mo 3 d oxidation states between the two catalysts during the...

X-ray photoelectron spectroscopy (XPS or ESCA) curve fitting procedures, reference materials and useful notes are listed here to provide a starting point for the consistent interpretation of XPS spectra.

The spin-orbit splitting of Mo 3d dipole into Mo 3d 3/2 and 3d 5/2 bands is observed in the XPS spectrum, which can be well fitted by two 3d doublets in the form of Gaussian functions ...

Figure 6 a and 6b show the Mo 3d core level XPS spectra of the in situ grown MoO 3 film (10 nm) before and after H 2 annealing, respectively. These two core level spectra were fitted...

In this work, we used a straightforward wet-chemistry method to synthesize plasmonic octahedral gold nanoparticles (NPs) coated with thin molybdenum oxide (MoO3-x), Au@MoO3-x NPs, which...

X-ray photoelectron spectroscopic (XPS) core-level spectra of MoO3/SiO thin films are presented. The effects of changes in composition, substrate temperature during deposition and annealing on the binding energy of Mo(3d) and Si(2p) core lines in …

X-ray photoelectron spectroscopy (XPS) core level spectra of MoO 3 substoichiometric amorphous thin films in the thickness range 100 to 670 nm were studied as a function of thickness. Some samples 500 nm thick were studied for different substrate temperatures in the range 293 to 543 K.